等离子旋转电极工艺粉末:综合指南

目录

概述

Plasma rotating electrode process (PREP) powder is a type of spherical powder made using the PREP method. PREP powders have unique properties that make them suitable for use in various applications like thermal spray coatings, metal additive manufacturing, and metal injection molding.

Some key features of PREP powder include:

  • Highly spherical morphology with smooth surface
  • Controlled microstructure with fine grain size
  • Low porosity and high density
  • Excellent flowability and spreadability
  • 包装密度高
  • Good blending characteristics
  • Capability to manufacture alloys and composites

PREP enables customization of powder characteristics like particle size distribution, composition, density, oxide content, and more. By controlling the PREP process parameters, powders can be engineered for specific application requirements.

Types of PREP Powders

粉末材料组成Key Properties and Applications
镍合金NiCr, NiCrAlY, NiCoCrAlYOxidation and corrosion resistance. Thermal spray coatings.
Cobalt alloyCoCr, CoCrAlY, CoNiCrAlYHigh temperature strength. Thermal spray coatings.
不锈钢316L, 304LCorrosion resistance. Metal AM, MIM.
工具钢H13, P20High hardness. Metal AM, MIM.
钛合金Ti6Al4V, TiAlHigh strength-to-weight ratio. Biomedical implants, aerospace.
铜合金CuCrZrHigh thermal conductivity. Electronic applications.
铝合金AlSi12Lightweight. Automotive components.
Tungsten alloyWNiFe, WCoHigh density. Radiation shielding.

Composition and Microstructure

PREP enables close control over powder composition and microstructural features:

  • Alloying elements can be modified to achieve desired properties
  • Microsegregation is minimized compared to gas atomization
  • Fine grained microstructure with uniform distribution of phases
  • Porosity and oxide content can be reduced to very low levels
  • Spherical morphology is maintained after alloying

Key Properties of PREP Powder

物业说明益处
粒径分布PREP can achieve narrow distribution with controlled d50.Ensures uniform melting and consistent properties.
形态学Highly spherical shape, smooth surface.Excellent flow and packing density.
表观密度Can be optimized based on requirements.Higher density improves powder spreading.
流动性Measured by Hall flowmeter method.Ensures uniform powder feeding and spreading.
Packing densityHigh packing density up to 60%.Maximizes volume fraction of metal powder in component.
氧化物含量Oxide levels below 0.2% achieved.Reduces oxide inclusions in final part.
微观结构Fine grained and homogeneous.Uniform property distribution in final part.
表面化学Chemistry precisely controlled.Oxide formation, wettability, and spreading optimized.

Applications of PREP Powder

PREP powder is used across various industries due to its specialized properties:

热喷涂涂层

  • Excellent flowability results in uniform feed rate and coating quality
  • Controlled particle size distribution optimizes melting and minimizes unmelted powder
  • Smooth surface morphology improves coating density and adhesion strength
  • Low oxide content prevents oxide inclusions in coating
  • Spherical shape gives higher deposition efficiency

金属 快速成型制造

  • High packing density allows more material per layer, reducing voids
  • Smooth surface morphology results in uniform melting and melt pool flow
  • Controlled particle size distribution prevents segregation issues
  • Low surface oxide enables good inter-particle bonding
  • Sphericity and flowability minimize powder feed problems

金属注射成型

  • High packing density maximizes sintered density
  • Uniform particle size distribution prevents segregation
  • Good flowability and compatibility results in homogenous mixing
  • Low oxide content prevents sintering defects
  • Controlled composition yields desired properties after sintering

规格

Typical specifications for PREP powder:

参数范围
颗粒大小10 - 150 微米
粒径分布D10, D50, D90 can be controlled
形态学Highly spherical ≥ 0.9
表观密度Up to 60% of theoretical density
Hall flowability< 30 s/50 g
氧化物含量< 0.2 wt%
微观结构Fine grained < 10 microns
表面化学O, C, N levels precisely controlled

供应商和定价

Some leading global suppliers of PREP powders are:

供应商地点
山特维克瑞典
普莱克斯美国
霍加纳斯瑞典
中石油粉体集团中国

Pricing for PREP powder varies based on:

  • Base metal (Ni, Co, steel)
  • 合金成分
  • 粒径分布
  • 订购数量
  • Level of customization

Indicative pricing ranges from $50/kg to $120/kg for common alloys. Custom alloys and particle size distribution can increase cost.

Comparison to Gas Atomized Powder

参数PREP Powder气体雾化粉末
粒子形状高度球形Irregular, satellites present
氧化物含量Very low <0.2%Typically 0.5-2%
孔隙率Near fully denseCan have 10-20% porosity
Alloy homogenity优秀Segregation prone
流动性非常好Lower due to satellites
Packing densityUp to 60%Typically 30-40%
表面化学Precisely controlledVariable based on process
费用更高Lower capital cost

Advantages of PREP Powder

  • Excellent spherical morphology for flowability
  • 可控粒度分布
  • Low porosity and oxide content
  • Alloy homogeneity and fine microstructure
  • Customizable composition and properties
  • High packing density for AM and MIM

Limitations of PREP Powder

  • Higher cost compared to gas atomized powder
  • Limited to smaller particle sizes, usually below 150 microns
  • Requires advanced process control and optimization
  • Limited production rate compared to gas atomization
  • Restricted to select base metals like Ni, Co, and steels

常见问题

Q: What is plasma rotating electrode process (PREP) powder?

A: PREP powder is a highly spherical metallic powder produced using the PREP method which involves rotating an electrode in a plasma arc under precise control to achieve desired powder characteristics.

Q: What materials can be made into PREP powder?

A: Common materials include nickel, cobalt, stainless steel, tool steel, titanium, aluminum, and copper alloys. Other alloys and composites are also possible through PREP.

Q: What are the key advantages of PREP powder?

A: Key advantages are excellent sphericity and flowability, controlled particle distribution, low porosity and oxides, fine and uniform microstructure, customizable composition, and high packing density.

Q: What is PREP powder used for?

A: Major applications are thermal spray coatings, metal additive manufacturing, and metal injection molding due to its specialized properties.

Q: How is PREP powder different from gas atomized powder?

A: PREP powder has superior sphericity, lower oxides, less porosity, more homogenous composition and microstructure compared to gas atomized powder.

Q: Is PREP powder more expensive than gas atomized powder?

A: Yes, PREP powder typically costs more due to higher process complexity and control involved. But it offers significant performance advantages over gas atomized powder.

Q: What particle size is available for PREP powder?

A: The usual range is 10 to 150 microns. Both smaller and larger sizes are possible but less common. Particle size distribution can also be controlled as per requirements.

Q: Does PREP powder have limited alloy options?

A: PREP is most established for nickel, cobalt and stainless steel alloys. But ongoing process development is expanding the alloy systems possible, including reactive materials like titanium and aluminum.

Q: Can PREP powder be customized for specific applications?

A: Yes, customization is a key benefit of PREP. Particle characteristics and alloy composition can be tailored to meet requirements for thermal spray, AM, MIM, etc.

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